Synthesis Of Cetyltrimethylammonium Chloride Ceramic Membrane Impregnated With Tio Removal Of Hexavalent Chromium(vi) Synthesis Of Cetyltrimethylammonium Chloride Coated Diatomite Impregnated With Tio2 Nanoparticles Diatomit

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In this study, manufacture of ceramic membranes modified by nanomaterials (Tio2) and CTAC wasrndone. Materials were synthesized by the application of the sol-gel method with respective amountsrnmeasured in the molar ratio of Ti: Ethanol: HCL: H2O as 1:15:0.3:5. The coating of Tio2 was done byrntwo methods. The first method involves coating the sample with the prepared sol and subsequentlyrnletting the gelation process to occur. The gel-coated ceramic was then calcinated at 550rnc resulting inrna Tio2 coated ceramic sample. The second method involves preparing Tio2 particles with the formed rn0rn0rnc resulting in Tio2 powders. Taking the newly formed Tio2 powder with Nitricrnacid (HNO3) in the ratio of 0.5 gm Tio2 powder: 10ml of HNo3; rigorous mixing for three hours hasrnyielded a solution. Whereby a second sample was Immersed and calcined at the previous temperature.rnThe prepared samples were then Immersed again in a solution formed by CTAC and water at a ratiornof 5gm:100ml. The coated samples where finally dried and prepared for the testing. Materialrncharacterization and filtration tests were conducted to check whether or not the samples werernacceptable. SEM/EDS Mapping as well as XRD tests was done to determine the morphology andrnphase composition of the manufactured material. Performance in the form of efficiency was alsornconducted by the use of filtration test as another form of characterization. The results obtainedrnconfirmed that the prepared membrane has met all the objectives of the study and has successfullyrnremoved hexavalent chromium from water solution. The calculated efficiency value of thernrespected modified and unmodified membranes has been found to be 73.01% for the unmodified rngel calcination at 550rnmembrane while Tio2 modified is found to be 80.05% and CTAC modified 85.44% respectively.

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Synthesis Of Cetyltrimethylammonium Chloride Ceramic Membrane Impregnated With Tio Removal Of Hexavalent Chromium(vi)  Synthesis Of Cetyltrimethylammonium Chloride Coated Diatomite Impregnated With Tio2 Nanoparticles Diatomit

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